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This document specifies a method for the determination of the boiling range distribution of petroleum products. The method is applicable to petroleum products and fractions with a final boiling point of 538 °C or lower at atmospheric pressure as determined by this document. This document does not apply to gasoline samples or gasoline components. The method is limited to products having a boiling range greater than 55 °C and having a vapour pressure sufficiently low to permit sampling at ambient temperature.
The document describes two procedures.
a) Procedure A allows a larger selection of columns and analysis conditions, such as packed and capillary columns as well as a thermal conductivity detector in addition to the flame ionization detector. Analysis times range from 14 min to 60 min.
b) Procedure B is restricted to only three capillary columns and requires no sample dilution. The analysis time is reduced to about 8 min.
Both procedures have been successfully applied to samples containing fatty acid methyl esters (FAME) up to 20 % (volume fraction).
NOTE For the purposes of this document, the terms '% (mass fraction)' and '% (volume fraction)' are used to represent the mass fraction (µ), the volume fraction (f) of a material.
Author | ISO/TC 28 Petroleum and related products, fuels and lubricants from natural or synthetic sources |
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Editor | ISO |
Document type | Standard |
Format | Paper |
Edition | 5 |
Number of pages | 39 |
Replace | ISO 3924:2016 |
Weight(kg.) | 0.1663 |
Year | 2019 |
Country | Switzerland |